# ------------------------------------------------------------------------------------------------------ # # Begin METADATA documentation # # METADATA Date: July 26, 2006 # METADATA Contact: Jeffrey D. Martin # U.S. Geological Survey # NAWQA Pesticide Synthesis Project # 5957 Lakeside Boulevard # Indianapolis, IN 46278-1996 # voice: (317) 290-3333 x148 # fax: (317) 290-3313 # email: jdmartin@usgs.gov # # ------------------------------------------------------------------------------------------------------ # # METADATA Data Description: # # Filename: appendix7a-5.data.txt # # The data provided herein are summary statistics of pesticide compounds in water, by land-use class, # for 186 stream-water sites summarized in appendix 7 of USGS Circular 1291, Pesticides in the Nation's # Streams and Ground Water, 1992-2001: The Quality of Our Nation's Waters # URL http://water.usgs.gov/nawqa/pnsp/pubs/circ1291/ # # ------------------------------------------------------------------------------------------------------ # # METADATA Basic documentation of dataset elements: # # Data Attributes: # # LU # METH # PCODE # PEST # MAXLTMDL # NSITES # NOBS # PDANY # PD.01 # PD.1 # PD1 # P50 # P75 # P90 # P95 # MAX # # Note: The row in the data file that follows the row of variable names describes the # width of the field and the data type. S or s indicates a text variable, # D or d indicates a date variable, and N or n indicates a numeric variable. # For example: 15s indicates a 0- to 15-character text variable whereas # 9N indicates a 0- to 9-digit numeric variable. # # # Attribute label: LU # # Attribute description: Drainage basin land-use class # # Code Description # ----- ----------------------------------------------------------------------------------- # agr Greater than 50% agricultural land and less than or equal to 5% urban land # und Less than or equal to 25% agricultural land and less than or equal to 5% urban land # urb Greater than 25% urban land and less than or equal to 25% agricultural land # mix All other combinations of land use # # # Attribute label: METH # # Attribute description: Analytical method # # Code Description # ---- -------------------------------------- # GCMS Gas chromatography/mass spectrometry # HPLC High performance liquid chromatography # # # Attribute label: PCODE # # Attribute description: Parameter code. The 5-digit number used to identify an analyte or other # variable in the USGS National Water Information System (NWIS) # # # Attribute label: PEST # # Attribute description: Common name of the pesticide/analyte # # # Attribute label: MAXLTMDL # # Attribute description: Maximum value of the long-term method detection level for 1992-2002, # in micrograms per liter # # # Attribute label: NSITES # # Attribute description: Number of stream-water sites in the land-use class # # # Attribute label: NOBS # # Attribute description: Number of stream-water samples in the land-use class # # # Attribute label: PDANY # # Attribute description: Time-weighted frequency of detection, at any concentration, # in percent # # # Attribute label: PD.01 # # Attribute description: Time-weighted frequency of detection, at concentrations greater than # or equal to 0.01 micrograms per liter, in percent # # # Attribute label: PD.1 # # Attribute description: Time-weighted frequency of detection, at concentrations greater than # or equal to 0.1 micrograms per liter, in percent # # # Attribute label: PD1 # # Attribute description: Time-weighted frequency of detection, at concentrations greater than # or equal to 1 micrograms per liter, in percent # # # Attribute label: P50 # # Attribute description: Time-weighted 50th percentile of concentration, in micrograms per liter # # # Attribute label: P75 # # Attribute description: Time-weighted 75th percentile of concentration, in micrograms per liter # # # Attribute label: P90 # # Attribute description: Time-weighted 90th percentile of concentration, in micrograms per liter # # # Attribute label: P95 # # Attribute description: Time-weighted 95th percentile of concentration, in micrograms per liter # # # Attribute label: MAX # # Attribute description: Maxmimum measured concentration, in micrograms per liter # # # # End METADATA documentation # # ------------------------------------------------------------------------------------------------------ LU METH PCODE PEST MAXLTMDL NSITES NOBS PDANY PD.01 PD.1 PD1 P50 P75 P90 P95 MAX 3s 4s 5s 23s 5n 5n 5n 6n 8s 6s 6s 6s 6s 6s 6s 7s agr GCMS 49260 Acetochlor 0.003 54 1113 29.87 21.95 5.86 1.65 ND 0.008 0.045 0.130 10.600 agr GCMS 46342 Alachlor 0.002 83 1996 40.07 26.72 5.68 1.14 ND 0.011 0.040 0.110 6.700 agr GCMS 39632 Atrazine 0.004 83 2009 89.93 82.13 43.37 8.74 0.073 0.210 0.800 2.400 201.000 agr GCMS 82686 Azinphos-methyl 0.020 83 1961 2.35 >=2.23 0.59 0.00 ND ND ND ND 0.540 agr GCMS 82673 Benfluralin 0.005 83 2014 0.82 0.00 0.00 0.00 ND ND ND ND 0.007 agr GCMS 04028 Butylate 0.001 83 1998 3.72 1.92 0.39 0.06 ND ND ND ND 1.400 agr GCMS 82680 Carbaryl 0.021 83 2006 10.05 >=5.90 0.82 0.06 ND ND 0.002 0.013 4.780 agr GCMS 82674 Carbofuran 0.010 83 2003 10.37 9.00 2.75 0.37 ND ND 0.004 0.044 7.000 agr GCMS 38933 Chlorpyrifos 0.003 83 1980 11.55 5.29 0.25 0.00 ND ND 0.004 0.010 0.220 agr GCMS 04041 Cyanazine 0.009 83 1994 44.02 38.87 12.22 2.81 ND 0.030 0.140 0.430 160.000 agr GCMS 82682 Dacthal 0.002 83 2008 12.67 3.28 0.98 0.26 ND ND 0.001 0.005 40.000 agr GCMS 34653 p,p'-DDE 0.001 83 2013 5.75 0.29 0.00 0.00 ND ND ND 0.002 0.062 agr GCMS 04040 Deethylatrazine 0.003 83 2000 79.36 60.06 11.84 0.24 0.016 0.050 0.128 0.216 3.030 agr GCMS 39572 Diazinon 0.003 83 1990 13.34 6.38 0.84 0.03 ND ND 0.005 0.014 3.800 agr GCMS 39381 Dieldrin 0.002 83 2002 3.61 1.81 0.00 0.00 ND ND ND ND 0.064 agr GCMS 82660 2,6-Diethylaniline 0.003 83 2005 2.39 0.07 0.00 0.00 ND ND ND ND 0.018 agr GCMS 82677 Disulfoton 0.011 83 2013 0.40 >=0.31 0.08 0.02 ND ND ND ND 3.340 agr GCMS 82668 EPTC 0.001 83 1995 15.70 8.20 1.58 0.32 ND ND 0.007 0.020 7.300 agr GCMS 82663 Ethalfluralin 0.005 83 2006 1.49 1.18 0.07 0.00 ND ND ND ND 0.130 agr GCMS 82672 Ethoprop 0.002 83 1996 2.90 1.86 0.25 0.00 ND ND ND ND 0.455 agr GCMS 04095 Fonofos 0.001 83 2004 3.85 2.18 0.24 0.02 ND ND ND ND 1.200 agr GCMS 34253 alpha-HCH 0.002 83 2001 0.35 0.17 0.00 0.00 ND ND ND ND 0.069 agr GCMS 39341 gamma-HCH 0.002 83 2001 1.02 0.63 0.00 0.00 ND ND ND ND 0.053 agr GCMS 82666 Linuron 0.018 83 2005 2.45 >=1.93 0.53 0.01 ND ND ND ND 1.400 agr GCMS 39532 Malathion 0.014 83 2013 5.50 >=3.80 0.26 0.00 ND ND ND 0.004 0.523 agr GCMS 39415 Metolachlor 0.006 83 2007 81.72 67.27 29.32 5.97 0.029 0.130 0.490 1.200 77.600 agr GCMS 82630 Metribuzin 0.003 83 1986 17.18 12.38 2.24 0.44 ND ND 0.013 0.037 6.610 agr GCMS 82671 Molinate 0.001 83 1997 10.89 8.81 4.57 1.93 ND ND 0.005 0.077 200.000 agr GCMS 82684 Napropamide 0.003 83 1994 4.19 3.27 0.48 0.00 ND ND ND ND 0.767 agr GCMS 39542 Parathion 0.005 83 2001 0.05 0.05 0.03 0.00 ND ND ND ND 0.141 agr GCMS 82667 Parathion-methyl 0.003 83 1997 0.93 0.88 0.18 0.00 ND ND ND ND 0.422 agr GCMS 82669 Pebulate 0.002 83 2001 1.16 0.59 0.12 0.00 ND ND ND ND 0.240 agr GCMS 82683 Pendimethalin 0.011 83 2000 6.14 >=5.03 0.89 0.05 ND ND ND 0.010 2.050 agr GCMS 82687 cis-Permethrin 0.003 83 2003 0.18 0.18 0.00 0.00 ND ND ND ND 0.019 agr GCMS 82664 Phorate 0.006 83 2003 0.08 0.08 0.01 0.00 ND ND ND ND 0.600 agr GCMS 04037 Prometon 0.007 83 2007 43.65 24.76 0.76 0.00 ND 0.010 0.020 0.035 0.250 agr GCMS 82676 Pronamide 0.002 83 2004 2.46 1.54 0.23 0.00 ND ND ND ND 0.275 agr GCMS 04024 Propachlor 0.005 83 2003 2.16 0.78 0.14 0.00 ND ND ND ND 0.511 agr GCMS 82679 Propanil 0.005 83 2006 1.47 0.93 0.35 0.02 ND ND ND ND 2.050 agr GCMS 82685 Propargite 0.011 83 1991 3.06 >=1.94 0.82 0.21 ND ND ND ND 20.000 agr GCMS 04035 Simazine 0.006 83 2009 58.16 42.23 7.46 1.07 0.006 0.024 0.074 0.175 5.760 agr GCMS 82670 Tebuthiuron 0.008 83 1983 21.17 11.89 2.52 0.18 ND ND 0.013 0.034 6.330 agr GCMS 82665 Terbacil 0.017 83 1997 2.80 >=2.26 0.17 0.00 ND ND ND ND 0.540 agr GCMS 82675 Terbufos 0.009 83 2004 0.05 0.05 0.02 0.00 ND ND ND ND 0.560 agr GCMS 82681 Thiobencarb 0.002 83 1994 4.21 3.20 1.03 0.22 ND ND ND ND 4.380 agr GCMS 82678 Triallate 0.001 83 2014 3.84 1.55 0.15 0.00 ND ND ND ND 0.650 agr GCMS 82661 Trifluralin 0.005 83 2005 12.93 4.22 0.15 0.00 ND ND 0.004 0.008 0.168 agr HPLC 49315 Acifluorfen 0.040 62 1466 3.67 1.82 0.08 ND ND ND ND 1.100 agr HPLC 49312 Aldicarb 0.100 62 1470 0.13 0.13 0.00 ND ND ND ND 0.510 agr HPLC 49313 Aldicarb sulfone 0.100 62 1469 0.00 0.00 0.00 ND ND ND ND ND agr HPLC 49314 Aldicarb sulfoxide 0.140 62 1470 0.13 >=0.13 0.05 ND ND ND ND 1.910 agr HPLC 38711 Bentazon 0.030 62 1466 16.55 7.40 1.14 ND ND 0.070 0.140 8.600 agr HPLC 04029 Bromacil 0.040 62 1470 1.68 1.43 0.03 ND ND ND ND 1.900 agr HPLC 49311 Bromoxynil 0.030 62 1466 0.66 0.27 0.00 ND ND ND ND 0.770 agr HPLC 61188 Chloramben methyl ester 0.110 62 1470 0.00 >=0.00 0.00 ND ND ND ND ND agr HPLC 49306 Chlorothalonil 0.070 62 1462 0.03 0.00 0.00 ND ND ND ND 0.290 agr HPLC 49305 Clopyralid 0.210 62 1465 0.00 >=0.00 0.00 ND ND ND ND ND agr HPLC 39732 2,4-D 0.080 62 1465 13.08 10.59 1.28 ND ND 0.110 0.270 15.000 agr HPLC 49304 Dacthal monoacid 0.040 62 1466 0.18 0.11 0.00 ND ND ND ND 0.430 agr HPLC 38746 2,4-DB 0.130 62 1466 0.06 >=0.02 0.00 ND ND ND ND 0.130 agr HPLC 38442 Dicamba 0.050 62 1466 1.39 0.87 0.08 ND ND ND ND 1.140 agr HPLC 49303 Dichlobenil 0.050 62 1470 0.32 0.00 0.00 ND ND ND ND 0.010 agr HPLC 49302 Dichlorprop 0.060 62 1466 0.42 0.27 0.00 ND ND ND ND 0.260 agr HPLC 49301 Dinoseb 0.040 62 1466 0.27 0.11 0.07 ND ND ND ND 1.000 agr HPLC 49300 Diuron 0.060 62 1469 12.90 7.23 1.37 ND ND 0.040 0.250 14.000 agr HPLC 49299 DNOC 0.130 62 1466 0.09 >=0.09 0.00 ND ND ND ND 0.190 agr HPLC 49297 Fenuron 0.030 62 1470 0.12 0.05 0.00 ND ND ND ND 0.100 agr HPLC 38811 Fluometuron 0.030 62 1470 6.04 4.34 0.98 ND ND ND 0.060 8.600 agr HPLC 49308 3-Hydroxycarbofuran 0.050 62 1470 0.00 0.00 0.00 ND ND ND ND ND agr HPLC 38482 MCPA 0.100 62 1466 1.41 1.17 0.00 ND ND ND ND 0.940 agr HPLC 38487 MCPB 0.130 62 1465 0.00 >=0.00 0.00 ND ND ND ND ND agr HPLC 38501 Methiocarb 0.030 62 1469 0.08 0.08 0.00 ND ND ND ND 0.100 agr HPLC 49296 Methomyl 0.240 62 1469 1.41 >=1.17 0.04 ND ND ND ND 1.000 agr HPLC 49294 Neburon 0.030 62 1470 0.07 0.00 0.00 ND ND ND ND 0.030 agr HPLC 49293 Norflurazon 0.021 62 1468 4.15 3.27 0.03 ND ND ND ND 1.240 agr HPLC 49292 Oryzalin 0.140 62 1470 0.49 >=0.26 0.11 ND ND ND ND 1.800 agr HPLC 38866 Oxamyl 0.080 62 1469 0.57 0.30 0.00 ND ND ND ND 0.160 agr HPLC 49291 Picloram 0.040 62 1465 0.00 0.00 0.00 ND ND ND ND ND agr HPLC 49236 Propham 0.110 62 1470 0.03 >=0.00 0.00 ND ND ND ND 0.060 agr HPLC 38538 Propoxur 0.060 62 1454 0.11 0.11 0.00 ND ND ND ND 0.110 agr HPLC 39742 2,4,5-T 0.040 62 1465 0.03 0.00 0.00 ND ND ND ND 0.050 agr HPLC 39762 2,4,5-TP 0.030 62 1465 0.00 0.00 0.00 ND ND ND ND ND agr HPLC 49235 Triclopyr 0.040 62 1466 2.17 1.76 0.30 ND ND ND ND 16.000 urb GCMS 49260 Acetochlor 0.003 23 549 3.38 2.52 0.67 0.00 ND ND ND ND 0.311 urb GCMS 46342 Alachlor 0.002 30 806 6.11 1.53 0.00 0.00 ND ND ND 0.004 0.092 urb GCMS 39632 Atrazine 0.004 30 801 70.73 47.19 10.19 1.48 0.009 0.027 0.100 0.209 3.370 urb GCMS 82686 Azinphos-methyl 0.020 30 804 0.48 >=0.48 0.36 0.00 ND ND ND ND 0.171 urb GCMS 82673 Benfluralin 0.005 30 814 3.41 0.53 0.00 0.00 ND ND ND ND 0.022 urb GCMS 04028 Butylate 0.001 30 811 0.16 0.00 0.00 0.00 ND ND ND ND 0.009 urb GCMS 82680 Carbaryl 0.021 30 808 49.47 >=41.59 14.15 1.27 ND 0.035 0.180 0.280 5.200 urb GCMS 82674 Carbofuran 0.010 30 811 1.59 1.23 0.00 0.00 ND ND ND ND 0.055 urb GCMS 38933 Chlorpyrifos 0.003 30 796 29.80 16.58 0.80 0.00 ND 0.006 0.018 0.034 0.300 urb GCMS 04041 Cyanazine 0.009 30 810 2.68 1.82 0.06 0.00 ND ND ND ND 0.132 urb GCMS 82682 Dacthal 0.002 30 813 23.16 3.26 0.00 0.00 ND ND 0.003 0.006 0.045 urb GCMS 34653 p,p'-DDE 0.001 30 812 2.02 0.00 0.00 0.00 ND ND ND ND 0.007 urb GCMS 04040 Deethylatrazine 0.003 30 802 42.33 12.20 1.05 0.00 ND 0.005 0.012 0.024 0.283 urb GCMS 39572 Diazinon 0.003 30 793 70.32 61.03 13.82 1.26 0.019 0.046 0.150 0.318 2.300 urb GCMS 39381 Dieldrin 0.002 30 809 3.29 3.24 0.00 0.00 ND ND ND ND 0.077 urb GCMS 82660 2,6-Diethylaniline 0.003 30 811 0.29 0.00 0.00 0.00 ND ND ND ND 0.006 urb GCMS 82677 Disulfoton 0.011 30 814 0.15 >=0.03 0.00 0.00 ND ND ND ND 0.018 urb GCMS 82668 EPTC 0.001 30 804 5.24 1.46 0.00 0.00 ND ND ND 0.001 0.038 urb GCMS 82663 Ethalfluralin 0.005 30 811 0.00 0.00 0.00 0.00 ND ND ND ND ND urb GCMS 82672 Ethoprop 0.002 30 807 0.91 0.29 0.06 0.00 ND ND ND ND 0.124 urb GCMS 04095 Fonofos 0.001 30 810 1.55 1.17 0.00 0.00 ND ND ND ND 0.084 urb GCMS 34253 alpha-HCH 0.002 30 812 0.00 0.00 0.00 0.00 ND ND ND ND ND urb GCMS 39341 gamma-HCH 0.002 30 803 3.11 1.34 0.00 0.00 ND ND ND ND 0.048 urb GCMS 82666 Linuron 0.018 30 810 0.23 >=0.23 0.16 0.00 ND ND ND ND 0.250 urb GCMS 39532 Malathion 0.014 30 811 16.96 >=14.54 2.44 0.00 ND ND 0.020 0.055 0.634 urb GCMS 39415 Metolachlor 0.006 30 814 46.09 22.00 2.80 0.74 ND 0.008 0.022 0.046 2.420 urb GCMS 82630 Metribuzin 0.003 30 775 6.76 5.64 1.26 0.00 ND ND ND 0.015 0.358 urb GCMS 82671 Molinate 0.001 30 810 0.89 0.70 0.00 0.00 ND ND ND ND 0.096 urb GCMS 82684 Napropamide 0.003 30 809 0.91 0.53 0.00 0.00 ND ND ND ND 0.040 urb GCMS 39542 Parathion 0.005 30 810 0.27 0.27 0.00 0.00 ND ND ND ND 0.052 urb GCMS 82667 Parathion-methyl 0.003 30 809 0.13 0.13 0.00 0.00 ND ND ND ND 0.061 urb GCMS 82669 Pebulate 0.002 30 812 0.20 0.20 0.00 0.00 ND ND ND ND 0.023 urb GCMS 82683 Pendimethalin 0.011 30 807 8.97 >=7.95 1.21 0.00 ND ND ND 0.019 0.372 urb GCMS 82687 cis-Permethrin 0.003 30 813 0.00 0.00 0.00 0.00 ND ND ND ND ND urb GCMS 82664 Phorate 0.006 30 810 0.00 0.00 0.00 0.00 ND ND ND ND ND urb GCMS 04037 Prometon 0.007 30 811 81.29 65.58 6.34 0.35 0.020 0.040 0.078 0.113 25.100 urb GCMS 82676 Pronamide 0.002 30 805 2.48 2.18 0.10 0.00 ND ND ND ND 0.131 urb GCMS 04024 Propachlor 0.005 30 811 1.02 0.06 0.00 0.00 ND ND ND ND 0.015 urb GCMS 82679 Propanil 0.005 30 813 1.49 0.79 0.00 0.00 ND ND ND ND 0.091 urb GCMS 82685 Propargite 0.011 30 805 0.19 >=0.19 0.00 0.00 ND ND ND ND 0.042 urb GCMS 04035 Simazine 0.006 30 812 64.72 47.65 13.78 3.00 0.008 0.042 0.151 0.340 9.030 urb GCMS 82670 Tebuthiuron 0.008 30 785 30.18 23.46 3.01 0.35 ND 0.009 0.032 0.070 2.830 urb GCMS 82665 Terbacil 0.017 30 806 2.09 >=1.80 0.00 0.00 ND ND ND ND 0.072 urb GCMS 82675 Terbufos 0.009 30 811 0.00 0.00 0.00 0.00 ND ND ND ND ND urb GCMS 82681 Thiobencarb 0.002 30 810 0.67 0.00 0.00 0.00 ND ND ND ND 0.009 urb GCMS 82678 Triallate 0.001 30 812 1.71 1.06 0.16 0.00 ND ND ND ND 0.352 urb GCMS 82661 Trifluralin 0.005 30 811 8.15 1.12 0.00 0.00 ND ND ND 0.003 0.037 urb HPLC 49315 Acifluorfen 0.040 19 521 0.31 0.00 0.00 ND ND ND ND 0.060 urb HPLC 49312 Aldicarb 0.100 19 525 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49313 Aldicarb sulfone 0.100 19 524 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49314 Aldicarb sulfoxide 0.140 19 524 0.00 >=0.00 0.00 ND ND ND ND ND urb HPLC 38711 Bentazon 0.030 19 521 0.10 0.00 0.00 ND ND ND ND 0.040 urb HPLC 04029 Bromacil 0.040 19 524 1.64 0.91 0.34 ND ND ND ND 1.550 urb HPLC 49311 Bromoxynil 0.030 19 521 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 61188 Chloramben methyl ester 0.110 19 524 0.00 >=0.00 0.00 ND ND ND ND ND urb HPLC 49306 Chlorothalonil 0.070 19 523 1.19 0.00 0.00 ND ND ND ND 0.080 urb HPLC 49305 Clopyralid 0.210 19 522 0.00 >=0.00 0.00 ND ND ND ND ND urb HPLC 39732 2,4-D 0.080 19 523 13.10 11.33 1.96 ND ND 0.160 0.450 5.530 urb HPLC 49304 Dacthal monoacid 0.040 19 521 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 38746 2,4-DB 0.130 19 523 0.09 >=0.09 0.00 ND ND ND ND 0.390 urb HPLC 38442 Dicamba 0.050 19 523 0.53 0.32 0.00 ND ND ND ND 0.160 urb HPLC 49303 Dichlobenil 0.050 19 525 3.72 0.69 0.10 ND ND ND ND 1.200 urb HPLC 49302 Dichlorprop 0.060 19 523 0.97 0.47 0.00 ND ND ND ND 0.320 urb HPLC 49301 Dinoseb 0.040 19 521 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49300 Diuron 0.060 19 525 22.35 14.23 2.59 ND ND 0.170 0.480 11.000 urb HPLC 49299 DNOC 0.130 19 522 0.32 >=0.32 0.00 ND ND ND ND 0.320 urb HPLC 49297 Fenuron 0.030 19 524 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 38811 Fluometuron 0.030 19 524 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49308 3-Hydroxycarbofuran 0.050 19 525 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 38482 MCPA 0.100 19 523 2.39 2.11 0.08 ND ND ND ND 1.300 urb HPLC 38487 MCPB 0.130 19 523 0.00 >=0.00 0.00 ND ND ND ND ND urb HPLC 38501 Methiocarb 0.030 19 524 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49296 Methomyl 0.240 19 524 0.13 >=0.13 0.00 ND ND ND ND 0.140 urb HPLC 49294 Neburon 0.030 19 524 0.35 0.00 0.00 ND ND ND ND 0.020 urb HPLC 49293 Norflurazon 0.021 19 524 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49292 Oryzalin 0.140 19 524 2.85 >=1.79 0.56 ND ND ND ND 1.900 urb HPLC 38866 Oxamyl 0.080 19 524 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49291 Picloram 0.040 19 520 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49236 Propham 0.110 19 525 0.75 >=0.00 0.00 ND ND ND ND 0.070 urb HPLC 38538 Propoxur 0.060 19 517 0.20 0.20 0.00 ND ND ND ND 0.260 urb HPLC 39742 2,4,5-T 0.040 19 521 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 39762 2,4,5-TP 0.030 19 521 0.00 0.00 0.00 ND ND ND ND ND urb HPLC 49235 Triclopyr 0.040 19 523 3.41 2.49 0.61 ND ND ND ND 3.350 und GCMS 49260 Acetochlor 0.003 7 121 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 46342 Alachlor 0.002 8 144 5.34 1.32 0.00 0.00 ND ND ND 0.002 0.010 und GCMS 39632 Atrazine 0.004 8 143 54.26 30.94 1.93 0.24 0.003 0.013 0.035 0.050 2.000 und GCMS 82686 Azinphos-methyl 0.020 8 141 0.99 >=0.99 0.00 0.00 ND ND ND ND 0.014 und GCMS 82673 Benfluralin 0.005 8 144 0.34 0.00 0.00 0.00 ND ND ND ND 0.002 und GCMS 04028 Butylate 0.001 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82680 Carbaryl 0.021 8 144 8.49 >=3.32 0.20 0.00 ND ND ND 0.007 0.432 und GCMS 82674 Carbofuran 0.010 8 144 2.07 1.64 0.24 0.00 ND ND ND ND 0.220 und GCMS 38933 Chlorpyrifos 0.003 8 144 3.07 0.22 0.00 0.00 ND ND ND ND 0.014 und GCMS 04041 Cyanazine 0.009 8 144 1.95 0.00 0.00 0.00 ND ND ND ND 0.009 und GCMS 82682 Dacthal 0.002 8 144 4.62 0.00 0.00 0.00 ND ND ND ND 0.005 und GCMS 34653 p,p'-DDE 0.001 8 144 2.17 0.00 0.00 0.00 ND ND ND ND 0.002 und GCMS 04040 Deethylatrazine 0.003 8 144 47.14 8.53 0.00 0.00 ND 0.005 0.010 0.011 0.040 und GCMS 39572 Diazinon 0.003 8 144 3.08 0.22 0.00 0.00 ND ND ND ND 0.040 und GCMS 39381 Dieldrin 0.002 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82660 2,6-Diethylaniline 0.003 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82677 Disulfoton 0.011 8 144 0.00 >=0.00 0.00 0.00 ND ND ND ND ND und GCMS 82668 EPTC 0.001 8 144 2.60 0.74 0.00 0.00 ND ND ND ND 0.044 und GCMS 82663 Ethalfluralin 0.005 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82672 Ethoprop 0.002 8 144 0.70 0.70 0.00 0.00 ND ND ND ND 0.019 und GCMS 04095 Fonofos 0.001 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 34253 alpha-HCH 0.002 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 39341 gamma-HCH 0.002 8 144 0.48 0.48 0.26 0.00 ND ND ND ND 0.130 und GCMS 82666 Linuron 0.018 8 144 0.00 >=0.00 0.00 0.00 ND ND ND ND ND und GCMS 39532 Malathion 0.014 8 144 3.45 >=0.00 0.00 0.00 ND ND ND ND 0.006 und GCMS 39415 Metolachlor 0.006 8 144 40.05 8.13 0.24 0.00 ND 0.004 0.009 0.019 0.500 und GCMS 82630 Metribuzin 0.003 8 143 2.23 2.23 0.26 0.00 ND ND ND ND 0.130 und GCMS 82671 Molinate 0.001 8 144 0.60 0.00 0.00 0.00 ND ND ND ND 0.005 und GCMS 82684 Napropamide 0.003 8 144 1.08 0.00 0.00 0.00 ND ND ND ND 0.008 und GCMS 39542 Parathion 0.005 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82667 Parathion-methyl 0.003 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82669 Pebulate 0.002 8 144 0.70 0.70 0.00 0.00 ND ND ND ND 0.085 und GCMS 82683 Pendimethalin 0.011 8 144 0.00 >=0.00 0.00 0.00 ND ND ND ND ND und GCMS 82687 cis-Permethrin 0.003 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82664 Phorate 0.006 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 04037 Prometon 0.007 8 144 17.29 1.28 0.00 0.00 ND ND 0.004 0.007 0.071 und GCMS 82676 Pronamide 0.002 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 04024 Propachlor 0.005 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82679 Propanil 0.005 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82685 Propargite 0.011 8 144 0.00 >=0.00 0.00 0.00 ND ND ND ND ND und GCMS 04035 Simazine 0.006 8 144 23.92 6.75 0.24 0.00 ND ND 0.008 0.013 0.140 und GCMS 82670 Tebuthiuron 0.008 8 143 21.32 13.28 0.00 0.00 ND ND 0.014 0.025 0.087 und GCMS 82665 Terbacil 0.017 8 144 0.70 >=0.70 0.00 0.00 ND ND ND ND 0.092 und GCMS 82675 Terbufos 0.009 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82681 Thiobencarb 0.002 8 144 0.00 0.00 0.00 0.00 ND ND ND ND ND und GCMS 82678 Triallate 0.001 8 144 1.08 1.08 0.00 0.00 ND ND ND ND 0.011 und GCMS 82661 Trifluralin 0.005 8 144 0.34 0.00 0.00 0.00 ND ND ND ND 0.001 und HPLC 49315 Acifluorfen 0.040 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49312 Aldicarb 0.100 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49313 Aldicarb sulfone 0.100 5 100 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49314 Aldicarb sulfoxide 0.140 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 38711 Bentazon 0.030 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 04029 Bromacil 0.040 5 101 0.85 0.85 0.00 ND ND ND ND 0.320 und HPLC 49311 Bromoxynil 0.030 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 61188 Chloramben methyl ester 0.110 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 49306 Chlorothalonil 0.070 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49305 Clopyralid 0.210 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 39732 2,4-D 0.080 5 101 0.38 0.00 0.00 ND ND ND ND 0.060 und HPLC 49304 Dacthal monoacid 0.040 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 38746 2,4-DB 0.130 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 38442 Dicamba 0.050 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49303 Dichlobenil 0.050 5 101 0.30 0.00 0.00 ND ND ND ND 0.080 und HPLC 49302 Dichlorprop 0.060 5 101 0.38 0.38 0.00 ND ND ND ND 0.180 und HPLC 49301 Dinoseb 0.040 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49300 Diuron 0.060 5 101 4.20 0.00 0.00 ND ND ND ND 0.020 und HPLC 49299 DNOC 0.130 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 49297 Fenuron 0.030 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 38811 Fluometuron 0.030 5 101 1.81 0.00 0.00 ND ND ND ND 0.080 und HPLC 49308 3-Hydroxycarbofuran 0.050 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 38482 MCPA 0.100 5 101 1.12 0.00 0.00 ND ND ND ND 0.020 und HPLC 38487 MCPB 0.130 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 38501 Methiocarb 0.030 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49296 Methomyl 0.240 5 100 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 49294 Neburon 0.030 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49293 Norflurazon 0.021 5 101 1.81 1.81 0.00 ND ND ND ND 0.170 und HPLC 49292 Oryzalin 0.140 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 38866 Oxamyl 0.080 5 100 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49291 Picloram 0.040 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49236 Propham 0.110 5 101 0.00 >=0.00 0.00 ND ND ND ND ND und HPLC 38538 Propoxur 0.060 5 100 0.00 0.00 0.00 ND ND ND ND ND und HPLC 39742 2,4,5-T 0.040 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 39762 2,4,5-TP 0.030 5 101 0.00 0.00 0.00 ND ND ND ND ND und HPLC 49235 Triclopyr 0.040 5 101 0.00 0.00 0.00 ND ND ND ND ND mix GCMS 49260 Acetochlor 0.003 51 1034 8.31 6.47 2.16 0.15 ND ND ND 0.020 1.660 mix GCMS 46342 Alachlor 0.002 65 1378 20.26 9.93 2.00 0.14 ND ND 0.010 0.021 3.800 mix GCMS 39632 Atrazine 0.004 65 1382 85.13 61.33 22.17 3.63 0.016 0.075 0.276 0.678 41.300 mix GCMS 82686 Azinphos-methyl 0.020 65 1354 1.83 >=1.26 0.03 0.00 ND ND ND ND 0.128 mix GCMS 82673 Benfluralin 0.005 65 1386 1.16 0.13 0.07 0.00 ND ND ND ND 0.205 mix GCMS 04028 Butylate 0.001 65 1383 1.62 0.36 0.00 0.00 ND ND ND ND 0.073 mix GCMS 82680 Carbaryl 0.021 65 1381 18.26 >=10.67 1.62 0.00 ND ND 0.012 0.029 0.672 mix GCMS 82674 Carbofuran 0.010 65 1371 3.99 3.12 0.50 0.09 ND ND ND ND 1.690 mix GCMS 38933 Chlorpyrifos 0.003 65 1366 17.23 7.31 0.24 0.00 ND ND 0.007 0.013 0.154 mix GCMS 04041 Cyanazine 0.009 65 1378 22.72 17.79 3.69 0.78 ND ND 0.031 0.059 5.100 mix GCMS 82682 Dacthal 0.002 65 1384 12.88 2.40 0.16 0.00 ND ND 0.001 0.003 0.179 mix GCMS 34653 p,p'-DDE 0.001 65 1383 6.68 0.07 0.00 0.00 ND ND ND 0.001 0.010 mix GCMS 04040 Deethylatrazine 0.003 65 1379 72.11 37.95 3.47 0.00 0.006 0.018 0.047 0.075 0.468 mix GCMS 39572 Diazinon 0.003 65 1353 36.87 23.57 2.33 0.03 ND 0.008 0.038 0.067 1.100 mix GCMS 39381 Dieldrin 0.002 65 1383 0.96 0.29 0.00 0.00 ND ND ND ND 0.015 mix GCMS 82660 2,6-Diethylaniline 0.003 65 1385 1.06 0.00 0.00 0.00 ND ND ND ND 0.008 mix GCMS 82677 Disulfoton 0.011 65 1386 0.06 >=0.06 0.06 0.00 ND ND ND ND 0.826 mix GCMS 82668 EPTC 0.001 65 1368 8.88 3.86 1.56 0.80 ND ND ND 0.007 29.600 mix GCMS 82663 Ethalfluralin 0.005 65 1385 0.29 0.11 0.00 0.00 ND ND ND ND 0.017 mix GCMS 82672 Ethoprop 0.002 65 1381 0.62 0.21 0.00 0.00 ND ND ND ND 0.052 mix GCMS 04095 Fonofos 0.001 65 1382 1.06 0.22 0.00 0.00 ND ND ND ND 0.014 mix GCMS 34253 alpha-HCH 0.002 65 1384 0.20 0.10 0.00 0.00 ND ND ND ND 0.014 mix GCMS 39341 gamma-HCH 0.002 65 1355 1.91 1.43 0.00 0.00 ND ND ND ND 0.043 mix GCMS 82666 Linuron 0.018 65 1382 0.80 >=0.74 0.31 0.00 ND ND ND ND 0.519 mix GCMS 39532 Malathion 0.014 65 1386 6.74 >=3.89 0.41 0.00 ND ND ND 0.006 0.670 mix GCMS 39415 Metolachlor 0.006 65 1386 68.13 45.40 9.80 1.49 0.008 0.029 0.099 0.240 16.400 mix GCMS 82630 Metribuzin 0.003 65 1359 6.59 5.93 1.51 0.12 ND ND ND 0.014 2.300 mix GCMS 82671 Molinate 0.001 65 1381 1.90 1.17 0.31 0.06 ND ND ND ND 1.570 mix GCMS 82684 Napropamide 0.003 65 1382 1.38 1.03 0.00 0.00 ND ND ND ND 0.054 mix GCMS 39542 Parathion 0.005 65 1384 0.15 0.08 0.00 0.00 ND ND ND ND 0.041 mix GCMS 82667 Parathion-methyl 0.003 65 1381 0.31 0.31 0.15 0.00 ND ND ND ND 0.521 mix GCMS 82669 Pebulate 0.002 65 1382 0.58 0.26 0.00 0.00 ND ND ND ND 0.021 mix GCMS 82683 Pendimethalin 0.011 65 1384 5.50 >=3.44 0.47 0.00 ND ND ND 0.005 0.266 mix GCMS 82687 cis-Permethrin 0.003 65 1385 0.53 0.07 0.00 0.00 ND ND ND ND 0.013 mix GCMS 82664 Phorate 0.006 65 1385 0.12 0.12 0.00 0.00 ND ND ND ND 0.033 mix GCMS 04037 Prometon 0.007 65 1386 55.41 36.55 4.84 0.08 0.004 0.019 0.049 0.099 1.950 mix GCMS 82676 Pronamide 0.002 65 1385 0.52 0.23 0.06 0.00 ND ND ND ND 0.430 mix GCMS 04024 Propachlor 0.005 65 1385 0.70 0.34 0.00 0.00 ND ND ND ND 0.064 mix GCMS 82679 Propanil 0.005 65 1384 0.44 0.17 0.00 0.00 ND ND ND ND 0.029 mix GCMS 82685 Propargite 0.011 65 1342 1.11 >=0.72 0.22 0.07 ND ND ND ND 2.000 mix GCMS 04035 Simazine 0.006 65 1385 63.42 43.66 6.63 0.64 0.007 0.026 0.071 0.159 1.620 mix GCMS 82670 Tebuthiuron 0.008 65 1354 28.65 15.20 0.20 0.00 ND 0.005 0.013 0.020 0.430 mix GCMS 82665 Terbacil 0.017 65 1381 5.27 >=4.88 0.51 0.00 ND ND ND 0.009 0.180 mix GCMS 82675 Terbufos 0.009 65 1386 0.27 0.20 0.00 0.00 ND ND ND ND 0.031 mix GCMS 82681 Thiobencarb 0.002 65 1383 1.01 0.58 0.06 0.00 ND ND ND ND 0.165 mix GCMS 82678 Triallate 0.001 65 1381 5.63 1.37 0.06 0.00 ND ND ND 0.002 0.118 mix GCMS 82661 Trifluralin 0.005 65 1384 10.39 1.60 0.00 0.00 ND ND 0.002 0.004 0.097 mix HPLC 49315 Acifluorfen 0.040 36 800 0.24 0.08 0.00 ND ND ND ND 0.390 mix HPLC 49312 Aldicarb 0.100 36 803 0.05 0.05 0.00 ND ND ND ND 0.480 mix HPLC 49313 Aldicarb sulfone 0.100 36 802 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 49314 Aldicarb sulfoxide 0.140 36 802 0.05 >=0.05 0.05 ND ND ND ND 1.200 mix HPLC 38711 Bentazon 0.030 36 800 3.76 2.15 0.07 ND ND ND ND 2.620 mix HPLC 04029 Bromacil 0.040 36 802 0.03 0.03 0.03 ND ND ND ND 4.000 mix HPLC 49311 Bromoxynil 0.030 36 800 0.17 0.00 0.00 ND ND ND ND 0.070 mix HPLC 61188 Chloramben methyl ester 0.110 36 801 0.00 >=0.00 0.00 ND ND ND ND ND mix HPLC 49306 Chlorothalonil 0.070 36 800 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 49305 Clopyralid 0.210 36 800 0.00 >=0.00 0.00 ND ND ND ND ND mix HPLC 39732 2,4-D 0.080 36 801 6.38 4.81 0.55 ND ND ND 0.080 1.400 mix HPLC 49304 Dacthal monoacid 0.040 36 800 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 38746 2,4-DB 0.130 36 801 0.13 >=0.05 0.00 ND ND ND ND 0.830 mix HPLC 38442 Dicamba 0.050 36 800 0.60 0.49 0.00 ND ND ND ND 0.250 mix HPLC 49303 Dichlobenil 0.050 36 799 0.40 0.00 0.00 ND ND ND ND 0.080 mix HPLC 49302 Dichlorprop 0.060 36 801 0.25 0.00 0.00 ND ND ND ND 0.090 mix HPLC 49301 Dinoseb 0.040 36 800 0.02 0.02 0.00 ND ND ND ND 0.270 mix HPLC 49300 Diuron 0.060 36 798 8.41 3.86 0.20 ND ND ND 0.060 4.150 mix HPLC 49299 DNOC 0.130 36 801 0.00 >=0.00 0.00 ND ND ND ND ND mix HPLC 49297 Fenuron 0.030 36 802 0.46 0.00 0.00 ND ND ND ND 0.050 mix HPLC 38811 Fluometuron 0.030 36 802 1.28 0.30 0.00 ND ND ND ND 0.630 mix HPLC 49308 3-Hydroxycarbofuran 0.050 36 802 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 38482 MCPA 0.100 36 801 1.30 0.98 0.21 ND ND ND ND 18.580 mix HPLC 38487 MCPB 0.130 36 801 0.15 >=0.00 0.00 ND ND ND ND 0.060 mix HPLC 38501 Methiocarb 0.030 36 802 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 49296 Methomyl 0.240 36 801 0.19 >=0.19 0.00 ND ND ND ND 0.270 mix HPLC 49294 Neburon 0.030 36 802 0.06 0.00 0.00 ND ND ND ND 0.040 mix HPLC 49293 Norflurazon 0.021 36 802 0.06 0.00 0.00 ND ND ND ND 0.040 mix HPLC 49292 Oryzalin 0.140 36 798 0.35 >=0.06 0.00 ND ND ND ND 0.130 mix HPLC 38866 Oxamyl 0.080 36 800 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 49291 Picloram 0.040 36 800 0.08 0.00 0.00 ND ND ND ND 0.010 mix HPLC 49236 Propham 0.110 36 802 0.00 >=0.00 0.00 ND ND ND ND ND mix HPLC 38538 Propoxur 0.060 36 800 0.20 0.11 0.00 ND ND ND ND 0.190 mix HPLC 39742 2,4,5-T 0.040 36 800 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 39762 2,4,5-TP 0.030 36 800 0.00 0.00 0.00 ND ND ND ND ND mix HPLC 49235 Triclopyr 0.040 36 801 0.24 0.13 0.13 ND ND ND ND 1.040